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Updated: Apr 15, 2026

Synthesis and Reaction Chemistry of Nanosize Monosodium Titanate
Published on: February 23, 2016
Rutile phase n- and p-type anodic titania nanotube arrays with square-shaped pore morphologies
Piyush Kar1, Yun Zhang, Samira Farsinezhad
1Department of Electrical and Computer Engineering, University of Alberta, Edmonton, Alberta T6G2 V4, Canada. pkar1@ualberta.ca.
Abstract:
Rutile-phase TiO2 nanotube arrays without broken walls were formed by annealing of anodically formed nanotubes in a propane flame at 650 °C and in air at 750 °C. An unusual morphological transformation was observed from the ellipsoidal pore-shapes of titania nanotubes grown in aqueous electrolyte to a square-shaped pore structure subsequent to the anneals. 750 °C annealed nanotubes were found to be lightly p-type, rare in TiO2.
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