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Updated: Mar 31, 2026

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Diffraction scattering computed tomography: a window into the structures of complex nanomaterials
M E Birkbak1, H Leemreize, S Frølich
1iNANO and Department of Chemistry, Aarhus University, 14 Gustav Wieds Vej, 8000 Aarhus, Denmark. hbirkedal@chem.au.dk.
Abstract:
Modern functional nanomaterials and devices are increasingly composed of multiple phases arranged in three dimensions over several length scales. Therefore there is a pressing demand for improved methods for structural characterization of such complex materials. An excellent emerging technique that addresses this problem is diffraction/scattering computed tomography (DSCT). DSCT combines the merits of diffraction and/or small angle scattering with computed tomography to allow imaging the interior of materials based on the diffraction or small angle scattering signals. This allows, e.g., one to distinguish the distributions of polymorphs in complex mixtures. Here we review this technique and give examples of how it can shed light on modern nanoscale materials.
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