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A new multipurpose diffractometer PILATUS@SNBL.

Vadim Dyadkin1, Philip Pattison2, Vladimir Dmitriev2

  • 1European Synchrotron Radiation Facility, 38000 Grenoble, France.

Journal of Synchrotron Radiation
|May 4, 2016
PubMed
Summary
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A new multifunctional diffractometer featuring a fast area detector and flexible goniometry is now available at the European Synchrotron Radiation Facility. This advanced setup enhances materials research with user-friendly control software and integrated auxiliary equipment.

Area of Science:

  • Materials Science
  • Crystallography
  • Synchrotron Radiation

Background:

  • The European Synchrotron Radiation Facility (ESRF) diffraction beamline BM01A has operated for 20 years.
  • Advancements in detector technology and user needs necessitate updated instrumentation.

Purpose of the Study:

  • To introduce and describe a new multifunctional diffractometer at the BM01A beamline.
  • To highlight the capabilities of the new Dectris Pilatus 2M detector and associated control system.

Main Methods:

  • Construction and commissioning of a new diffractometer system.
  • Integration of a Dectris Pilatus 2M area detector with tilt and translation capabilities.
  • Implementation of user-friendly graphical user interface (GUI) software (Pylatus) for instrument control.
Keywords:
area detectordata processingdiffractometry

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Main Results:

  • A novel diffractometer combining a fast, low-noise area detector with flexible goniometry has been successfully implemented.
  • The Pylatus software provides intuitive control over the diffractometer and auxiliary equipment.
  • The system supports various sample environments, including heating/cooling devices and in situ cells.

Conclusions:

  • The new diffractometer enhances the capabilities of the BM01A beamline for advanced materials research.
  • The integrated system offers improved experimental flexibility and user accessibility.
  • This upgrade supports diverse in situ studies and complementary spectroscopic analyses.