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Updated: Mar 21, 2026

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
Published on: June 19, 2018
A Johann-type X-ray emission spectrometer at the Rossendorf beamline
Kristina O Kvashnina1, Andreas C Scheinost1
1Rossendorf Beamline at ESRF - The European Synchrotron, CS40220, 38043 Grenoble Cedex 9, France.
Abstract:
This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.
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