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Updated: Mar 17, 2026

Quantitative Hardness Measurement by Instrumented AFM-indentation
Published on: November 22, 2016
Effect of Loading Rate Upon Conventional Ceramic Microindentation Hardness
George D Quinn1, Parimal J Patel2, Isabel Lloyd3
1National Institute of Standards and Technology, Gaithersburg, MD 20899-8521.
Abstract:
The world standards for conventional ceramic hardness have varying requirements for control of loading rate during the indentation cycle. A literature review suggests that loading rate may affect measured hardness in some instances. In view of the uncertainty over this issue, new experiments over a range of indentation loading rates were performed on a steel, sintered silicon carbide, and an aluminum oxynitride. There was negligible effect upon Vickers hardness when loading rate was varied by almost four orders of magnitude from approximately 0.03 N/s to 10 N/s.
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