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Updated: Mar 5, 2026

Synthesis and Characterization of Fe-doped Aluminosilicate Nanotubes with Enhanced Electron Conductive Properties
Published on: November 15, 2016
A Novel Fluoride Route for the Synthesis of Aluminosilicate Nanotubes
Atika Chemmi1, Jocelyne Brendlé2, Claire Marichal3
1Equipe Matériaux à Porosité Controlée (MPC), Institut de Science des Matériaux de Mulhouse (IS2M), CNRS UMR 7361, Université de Haute Alsace (UHA), ENSCMu, 3b rue Alfred Werner, 68093 Mulhouse Cedex, France. atika.chemmi@uha.fr.
Abstract:
In this work we present a novel method for synthesis of aluminosilicate nanotubes: the fluoride route. F-containing imogolite (F-IMO) exhibits an improved crystallization rate and improved yield. The structure of F-IMO was investigated and compared with F-free imogolite (IMO) by means of X-ray diffraction (XRD) and Fourier transformed infrared spectroscopy (FTIR) confirming imogolite structure. Solid state nuclear magnetic resonance (NMR) analyses show an increased crystallization rate for F-IMO and confirm the incorporation of fluorine ion in the structure.

