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Updated: Feb 27, 2026

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Scalable Syntheses of Graphene Oxide and Reduced Graphene Oxide using Cascade Design Oxidation and Highly Basic Reduction Reactions
Published on: July 3, 2025
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From graphite to interconnected reduced graphene oxide: one-pot synthesis and supercapacitor application
Boopathi Sidhureddy1, Antony Raj Thiruppathi, Aicheng Chen
1Department of Chemistry, Lakehead University, 955 Oliver Road, Thunder Bay, ON P7B 5E1, Canada. achen@lakeheadu.ca.
Summary
A streamlined Hummers method (SHM) enables scalable, one-pot production of interconnected reduced graphene oxide (IC-RGO). This novel 3D graphene platform offers potential in energy, environmental, and medical fields.
Area of Science:
- Materials Science
- Nanotechnology
- Chemical Engineering
Background:
- Graphene oxide (GO) and reduced graphene oxide (RGO) are crucial nanomaterials.
- Existing RGO production methods face challenges in scalability and structural control.
- Developing 3D graphene architectures is vital for advanced applications.
Purpose of the Study:
- To demonstrate an innovative one-pot method for scalable production of interconnected reduced graphene oxide (IC-RGO).
- To introduce the streamlined Hummers method (SHM) for synthesizing a novel 3D graphene platform.
- To highlight the potential applications of the synthesized IC-RGO.
Main Methods:
- Development of the streamlined Hummers method (SHM) for one-pot synthesis.
- Scalable production of interconnected reduced graphene oxide (IC-RGO).
- Characterization of the 3D graphene structure and properties (details not provided in abstract).
Main Results:
- Successful demonstration of a novel one-pot synthesis approach.
- Production of interconnected reduced graphene oxide (IC-RGO) on a scalable level.
- Formation of a new type of three-dimensional graphene platform.
Conclusions:
- The streamlined Hummers method (SHM) provides an efficient route for scalable IC-RGO production.
- The resulting IC-RGO serves as a promising 3D platform.
- Potential applications span energy storage, environmental remediation, and biomedical engineering.

