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Quantifying the Pathway and Predicting Spontaneous Emulsification during Material Exchange in a Two Phase Liquid

Stephen Spooner1, Alireza Rahnama2, Jason M Warnett2

  • 1WMG, University of Warwick, Coventry, CV4 7AL, UK. s.spooner@warwick.ac.uk.

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Summary

This study quantifies interfacial area changes in liquid metal-molten oxide systems, crucial for high-temperature manufacturing. It presents a method to predict and engineer microemulsion formation for streamlined processing.

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Area of Science:

  • Materials Science and Engineering
  • Chemical Engineering
  • Physical Chemistry

Background:

  • Kinetic control over thermodynamically favorable equilibria is key in materials processing.
  • Interfacial instability in systems with rapid material exchange is critical for manufacturing efficiency.
  • High-temperature systems benefit significantly from understanding transient interfacial area dynamics.

Purpose of the Study:

  • To quantify the physical pathway of interfacial area change in liquid metal-molten oxide systems.
  • To predict growth regimes and emulsification behavior using phase-field modeling.
  • To develop a method for predicting and engineering microemulsion formation.

Main Methods:

  • Quantification of interfacial area change during material exchange.
  • Phase-field modeling to predict growth regimes and emulsification.
  • In-situ observation of emulsification behavior to validate simulations.

Main Results:

  • The study presents a quantified pathway for interfacial area change in liquid metal-molten oxide systems.
  • Phase-field modeling successfully predicted growth regimes and emulsification behavior.
  • Observed emulsification behavior quantitatively validated the simulation of interfacial phenomena.

Conclusions:

  • A method is presented to predict and engineer microemulsion formation to specific requirements.
  • Understanding interfacial dynamics is crucial for optimizing high-temperature manufacturing processes.
  • The developed simulation method provides a tool for controlling microemulsion characteristics.