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Silicon(IV) Corroles.

Giuseppe Pomarico1, Donato Monti1, Martina Bischetti1

  • 1Department of Chemical Science and Technologies, University of Rome Tor Vergata, Via della Ricerca Scientifica snc, 00133, Rome, Italy.

Chemistry (Weinheim an Der Bergstrasse, Germany)
|April 12, 2018
PubMed
Summary
This summary is machine-generated.

New silicon corrole complexes were synthesized for the first time. These stable, luminescent silicon-corrole materials show potential as naked-eye sensors for fluoride detection.

Keywords:
luminescencemacrocyclic ligandsporphyrinoidssensorssilicon

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Area of Science:

  • Organometallic Chemistry
  • Materials Science
  • Supramolecular Chemistry

Background:

  • Corroles are macrocyclic ligands structurally related to porphyrins.
  • Silicon-porphyrin complexes have shown interesting photophysical and chemical properties.

Purpose of the Study:

  • To synthesize and characterize novel silicon-corrole complexes.
  • To investigate the stability, luminescence, and sensing capabilities of these complexes.

Main Methods:

  • Reaction of free-base corroles with hexachlorodisilane.
  • Characterization of products using spectroscopic techniques.
  • Evaluation of hydrolysis stability and luminescence properties.
  • Testing as fluoride sensors.

Main Results:

  • First synthesis of silicon corrole complexes achieved.
  • Peripheral substituents influence product formation (μ-oxo dimer or hydroxo complex).
  • Silicon corrole complexes exhibit enhanced hydrolytic stability and luminescence compared to porphyrins.
  • Demonstrated potential as naked-eye sensors for fluoride detection due to color changes.

Conclusions:

  • Peripheral group modification allows control over silicon corrole complex formation.
  • Silicon corroles are stable, luminescent materials with practical applications.
  • These complexes are promising candidates for sensitive and selective fluoride ion sensing.