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Bonding in Metals02:32

Bonding in Metals

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Metallic bonds are formed between two metal atoms. A simplified model to describe metallic bonding has been developed by Paul Drüde called the “Electron Sea Model”. 
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Metallic Solids02:37

Metallic Solids

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Metallic solids such as crystals of copper, aluminum, and iron are formed by metal atoms. The structure of metallic crystals is often described as a uniform distribution of atomic nuclei within a “sea” of delocalized electrons. The atoms within such a metallic solid are held together by a unique force known as metallic bonding that gives rise to many useful and varied bulk properties.
All metallic solids exhibit high thermal and electrical conductivity, metallic luster, and malleability....
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Alkali Metals03:06

Alkali Metals

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Group 1 elements are soft and shiny metallic solids. They are malleable, ductile, and good conductors of heat and electricity. The melting points of the alkali metals are unusually low for metals and decrease going down the group, while the density increases going down the group with the exception of potassium (Table 1).
Table 1: Properties of the alkali metals
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Metal-Ligand Bonds02:51

Metal-Ligand Bonds

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The hemoglobin in the blood, the chlorophyll in green plants, vitamin B-12, and the catalyst used in the manufacture of polyethylene all contain coordination compounds. Ions of the metals, especially the transition metals, are likely to form complexes.
In these complexes, transition metals form coordinate covalent bonds, a kind of Lewis acid-base interaction in which both of the electrons in the bond are contributed by a donor (Lewis base) to an electron acceptor (Lewis acid). The Lewis acid in...
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Properties of Transition Metals02:58

Properties of Transition Metals

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Transition metals are defined as those elements that have partially filled d orbitals. As shown in Figure 1, the d-block elements in groups 3–12 are transition elements. The f-block elements, also called inner transition metals (the lanthanides and actinides), also meet this criterion because the d orbital is partially occupied before the f orbitals.
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Theory of Metallic Conduction01:17

Theory of Metallic Conduction

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The conduction of free electrons inside a conductor is best described by quantum mechanics. However, a classical model makes predictions close to the results of quantum mechanics. It is called the theory of metallic conduction.
In this theory, Newton's second law of motion is used to determine the acceleration of an electron in the presence of an applied electric field. Then, its velocity is expressed via this acceleration.
An electron moves through the crystal, containing positive ions,...
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Related Experiment Video

Updated: Feb 7, 2026

Frugal Imaging Technique of Capillary Flow Through Three-Dimensional Polymeric Printing Powders
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Frugal Imaging Technique of Capillary Flow Through Three-Dimensional Polymeric Printing Powders

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Automated 3D EBSD for metallic powders.

Caitlin Walde1, Roger Ristau2, Danielle Cote1

  • 1Worcester Polytechnic Institute, United States.

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|July 13, 2018
PubMed
Summary
This summary is machine-generated.

This study presents a novel method for analyzing metallic powders before additive manufacturing. Understanding powder microstructure, particularly grain structure, can enhance final material properties.

Keywords:
3D microscopy3D sectioningAdditive manufacturingAutomated 3D-EBSD for metallic powders using a Xe P-FIBCharacterizationElectron microscopyMetallographyPowder metallurgySerial sectioningThree-dimensional microscopy

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Area of Science:

  • Materials Science
  • Metallurgy
  • Additive Manufacturing

Background:

  • Metallic powders are crucial for additive manufacturing, but their pre-consolidation properties are understudied.
  • Characterizing powder microstructure, specifically 3D grain structure, can predict bulk material properties.
  • Existing methods for analyzing bulk materials are difficult to apply to small powder particles.

Purpose of the Study:

  • To develop and recommend a method for preparing and analyzing metallic powder particles.
  • To enable detailed characterization of powder microstructure prior to additive manufacturing.
  • To facilitate fine-tuning of additively manufactured material properties through powder analysis.

Main Methods:

  • Utilized a Xenon Plasma Focused Ion Beam (Xe P-FIB) for serial sectioning and imaging.
  • Adapted bulk material milling and imaging techniques for individual metallic powder particles.
  • Developed specific methods for fixturing powder samples and protecting them during milling.

Main Results:

  • Successfully demonstrated a method for preparing and imaging metallic powder particles.
  • Enabled Electron Backscatter Diffraction (EBSD) measurements on individual powder particles.
  • Provided insights into the 3D grain structure of metallic powders.

Conclusions:

  • The developed Xe P-FIB method allows for detailed microstructural analysis of metallic powders.
  • This technique overcomes challenges in preparing and analyzing small powder particles.
  • Characterizing powder microstructure is key to optimizing additive manufacturing processes and material outcomes.