Characterization of pulp derived nanocellulose hydrogels using AVAP® technology.
Stuart Kyle1, Zita M Jessop1, Ayesha Al-Sabah2
1Reconstructive Surgery & Regenerative Medicine Group (ReconRegen), Institute of Life Sciences, Swansea University Medical School, Swansea, SA2 8PP, UK; The Welsh Centre for Burns and Plastic Surgery, Morriston Hospital, Swansea, SA6 6NL, UK.
Carbohydrate Polymers
|August 11, 2018
Summary
Researchers developed nanocellulose materials from wood biomass. These advanced nanocellulose (NC) materials exhibit unique structures and properties, showing potential for biomaterial applications.
Area of Science:
- Materials Science
- Biotechnology
- Nanotechnology
Background:
- Bioinspiration from natural hierarchical structures drives advanced functional material development.
- Nanocellulose (NC) is gaining attention for high-performance materials with tunable properties.
Purpose of the Study:
- To prepare and characterize nanocellulose fibrils, nanocrystals, and a novel blend from softwood biomass.
- To investigate the microarchitecture, porosity, and mechanical properties of these nanocellulose variants.
Main Methods:
- Preparation of nanocellulose using AVAP® biorefinery technology.
- Characterization via electron microscopy (SEM, TEM, AFM), FTIR, XRD, thermal analysis, surface charge, and rheology.
Main Results:
- All nanocellulose forms displayed nano- and microarchitectures with porosity, except for nanocrystals with compact nanorod packing.
- The NC blend showed porous fibrillar networks with interconnecting nanorods.
- Materials confirmed as pure cellulose I, exhibiting excellent thermal stability and stable colloidal suspensions. Rheology indicated dominant elasticity, with the NC blend being more rigid.
Conclusions:
- The developed nanocellulose materials possess distinct microarchitectures and tunable properties.
- The NC blend's unique structure suggests a double network hydrogel.
- These materials show significant potential for biomaterial applications requiring controlled microarchitecture, topography, and porosity.
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