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Updated: Feb 5, 2026

A Scalable Balz-Schiemann Reaction Protocol in a Continuous Flow Reactor
Published on: February 10, 2023
Heating-up control with delay-free output prediction for industrial jacketed reactors based on step response
Tao Liu1, Hongyu Tian1, Shili Rong1
1Institute of Advanced Control Technology, Dalian University of Technology, Dalian, 116024, PR China.
A new predictor-based two-degree-of-freedom (2DOF) control strategy improves heating control in industrial reactors. This method uses a identified process model to enhance temperature regulation performance, even with long delays.
Area of Science:
- Chemical Engineering
- Process Control
- Automation
Background:
- Industrial jacketed reactors often exhibit long input delays, complicating precise temperature control during heating-up phases.
- Existing control methods struggle to maintain optimal performance under these challenging dynamic conditions.
Purpose of the Study:
- To propose a novel predictor-based two-degree-of-freedom (2DOF) control scheme for enhancing heating-up control performance in industrial jacketed reactors.
- To develop a robust model identification method for accurately characterizing the reactor's thermal dynamics, including time delays.
Main Methods:
- A simple step response test was conducted to identify a transfer function model, representing an integrating process with time delay.
- A predictor-based 2DOF control structure was designed, utilizing two filters for delay-free output prediction.
- Controllers were analytically derived for set-point tracking and load disturbance rejection, featuring a single tunable parameter for performance optimization.
Main Results:
- The proposed identification method successfully established an accurate process model for the heating-up dynamics.
- The predictor-based 2DOF control scheme demonstrated effective temperature regulation and disturbance rejection capabilities.
- Validation through illustrative examples and a practical application on a 4-liter jacketed reactor confirmed the method's effectiveness.
Conclusions:
- The predictor-based 2DOF control strategy offers a significant improvement over existing methods for heating-up control in industrial reactors with long delays.
- The developed model identification and control design provide a tunable and effective solution for pharmaceutical crystallization and similar processes.
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