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Quality Control01:05

Quality Control

2.5K
Quality control is one of the three cyclical quality assurance activities that help keep a system under statistical control. Typical quality control activities include creating quality control charts, conducting proficiency testing, and documenting and archiving results.
Quality control helps track data, visualize trends, and identify variations, making it easier to detect deviations that may affect the accuracy of an analysis. One way to do this is by generating a quality control chart, which...
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Measurement: Standard Units03:38

Measurement: Standard Units

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Every measurement provides three kinds of information: the size or magnitude of the measurement (a number), a standard of comparison for the measurement (a unit), and an indication of the uncertainty of the measurement. While the number and unit are explicitly represented when a quantity is written, the uncertainty is an aspect of the errors in the measurement results.
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Units and Standards of Measurement01:10

Units and Standards of Measurement

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A physical quantity is defined either by specifying its measurement method or by stating how it is calculated from other measurements. For example, consider a metallic cube. We might define its mass and dimensions by specifying methods for measuring them, such as using a weighing machine and a meter scale. Then, we could define the volume by stating that it is the cube of its side, and we could calculate the density as the mass divided by the volume.
Measurements of physical quantities are...
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Electrophilic 1,2- and 1,4-Addition of X2 to 1,3-Butadiene01:14

Electrophilic 1,2- and 1,4-Addition of X2 to 1,3-Butadiene

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Electrophilic addition of halogens to alkenes proceeds via a cyclic halonium ion to form a 1,2-dihalide or a vicinal dihalide.
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Base-Catalyzed Aldol Addition Reaction01:08

Base-Catalyzed Aldol Addition Reaction

4.6K
As depicted in Figure 1, base-catalyzed aldol addition involves adding two carbonyl compounds in aqueous sodium hydroxide to form a β-hydroxy carbonyl compound.
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Conjugate Addition (1,4-Addition) vs Direct Addition (1,2-Addition)01:27

Conjugate Addition (1,4-Addition) vs Direct Addition (1,2-Addition)

4.3K
α,β-Unsaturated carbonyl compounds with two electrophilic sites, the carbonyl carbon, and the β carbon, are susceptible to nucleophilic attack via two modes: conjugate or 1,4-addition and direct or 1,2-addition.
Conjugate addition results in a thermodynamically stable product. The reaction retains the stronger C=O bond at the expense of the weaker C=C π bond. The process is slow as the β carbon is less electrophilic than the carbonyl carbon.
Direct addition products are...
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Manufacturing, Control, and Performance Evaluation of a Gecko-Inspired Soft Robot
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Standard method for microCT-based additive manufacturing quality control 2: Density measurement.

Anton du Plessis1, Philip Sperling2, Andre Beerlink2

  • 1CT Scanner Facility, Stellenbosch University, Stellenbosch, South Africa.

Methodsx
|October 9, 2018
PubMed
Summary

MicroComputed Tomography (MicroCT) can accurately measure average density by combining volumetric measurements with mass. This method integrates density analysis with 3D visualization of porosity and defects in the same sample.

Keywords:
Additive manufacturingDensityMicroCTNon-destructive testingStandard method for microCT-based additive manufacturing quality control 2: density measurementStandardizationX-rayTomography

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Area of Science:

  • Materials Science
  • Metrology
  • Non-destructive Testing

Background:

  • MicroComputed Tomography (MicroCT) is primarily recognized for porosity and defect quantification.
  • Accurate volumetric measurements are achievable with MicroCT, enabling density calculations.

Purpose of the Study:

  • To present a standardized MicroCT-based method for accurate mean density measurement.
  • To highlight the advantage of combining density analysis with other MicroCT-derived sample characteristics.

Main Methods:

  • Utilizing a 10 mm cube sample for standardized workflow.
  • Employing a laboratory MicroCT scanner with 15 μm voxel size.
  • Using software for sub-voxel precise edge determination for accurate volume measurement.
  • Combining accurate volume data with precise scale mass measurements.

Main Results:

  • Achieved accurate mean density measurements from scanned samples.
  • Enabled simultaneous analysis of density, porosity, void distribution, and surface roughness from a single scan.
  • Demonstrated the detection of internal features like unconsolidated powder, open porosity, and inclusions.

Conclusions:

  • The presented MicroCT density method offers a standardized and automated workflow.
  • This approach provides a comprehensive analysis of material properties, integrating density with structural characterization.
  • MicroCT is a versatile tool for both defect analysis and precise material property determination.