Related Experiment Video
Updated: Jan 30, 2026

High Pressure Single Crystal Diffraction at PX^2
Published on: January 16, 2017
Investigation of Grain Refinement Mechanism of Nickel Single Crystal during High Pressure Torsion by Crystal
Peitang Wei1, Hao Zhou2, Huaiju Liu3
1State Key Laboratory of Mechanical Transmissions, Chongqing University, Chongqing 400044, China. peitangwei@cqu.edu.cn.
Abstract:
The excellent properties of ultra-fine grained (UFG) materials are relevant to substantial grain refinement and the corresponding induced small grains delineated by high-angle grain boundaries. The present study aims to understand the grain refinement mechanism by examining the nickel single crystal processed by high pressure torsion (HPT), a severe plastic deformation method to produce UFG materials based upon crystal plasticity finite element (CPFEM) simulations. The predicted grain maps by the developed CPFEM model are capable of capturing the prominent characteristics associated with grain refinement in HPT. The evolution of the orientation of structural elements and the rotations of crystal lattices during the HPT process of the detected differently oriented grains are extensively examined. It has been found that there are mainly two intrinsic origins of lattice rotation which cause the initial single crystal to subdivide. The correlation between the crystallographic orientation changes and lattice rotations with the grain fragmentation are analyzed and discussed in detail based on the theory of crystal plasticity.
Related Concept Videos
Ionic Crystal Structures
Most monatomic ions behave as charged spheres, and their attraction for ions of opposite charge is the same in every direction. Consequently, stable structures for ionic compounds result (1) when ions of one charge are surrounded by as many ions as possible of the opposite...
Crystal Field Theory - Octahedral Complexes
To explain the observed behavior of transition metal complexes (such as colors), a model involving electrostatic interactions between the electrons from the ligands and the electrons in the unhybridized d orbitals of the central metal atom has been developed. This electrostatic model is crystal field theory (CFT). It helps to understand, interpret, and predict the colors, magnetic behavior, and some structures of coordination compounds of transition metals.
CFT focuses on...
Crystal Growth: Principles of Crystallization
Initiating crystallization involves manipulating the concentration of the solute and the temperature of the solution. Since crystal growth occurs when the ratio of concentration and solubility of the solute in the solvent...
Crystal Field Theory - Tetrahedral and Square Planar Complexes
Crystal field theory (CFT) is applicable to molecules in geometries other than octahedral. In octahedral complexes, the lobes of the dx2−y2 and dz2 orbitals point directly at the ligands. For tetrahedral complexes, the d orbitals remain in place, but with only four ligands located between the axes. None of the orbitals points directly at the tetrahedral ligands. However, the dx2−y2 and dz2 orbitals (along the Cartesian axes) overlap with the ligands less than the dxy,...
Torsion of Noncircular Members
Plastic Deformations of Members with a Single Plane of Symmetry

