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Quantitative Analysis of Vacuum Induction Melting by Laser-induced Breakdown Spectroscopy
Published on: June 10, 2019
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Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
Michele Calandri1, Shuo Yin2, Barry Aldwell3,4
1Dipartimento di Scienza Applicata e Tecnologia (DISAT), Politecnico di Torino, Corso Duca degli Abruzzi, 24, 10129 Turin, Italy. michele.calandri@polito.it.
Materials (Basel, Switzerland)
|April 24, 2019
Summary
Selective laser melting (SLM) of Inconel 718 creates a complex microstructure. Understanding this as-built material
Area of Science:
- Materials Science
- Metallurgy
- Additive Manufacturing
Background:
- Inconel 718 is suitable for selective laser melting (SLM).
- The SLM process results in a complex and heterogeneous microstructure in Inconel 718.
- Understanding the as-built microstructure is crucial for effective post-processing heat treatments.
Purpose of the Study:
- To investigate the microstructural features of as-built SLM Inconel 718 at multiple length scales.
- To analyze grain morphology and crystallographic texture.
- To understand the solidification mechanism and its impact on microstructure.
Main Methods:
- Optical Microscopy (OM)
- Scanning Electron Microscopy (SEM)
- Transmission Electron Microscopy (TEM)
- Electron Backscatter Diffraction (EBSD)
Main Results:
- Observed elongated grains in the build direction, unaffected by laser tracks or melt pools, indicating epitaxial growth.
- Identified columnar dendrites within grains, aligned with the thermal gradient along <100> axes.
- Detected microsegregation, interdendritic precipitates, and dislocations at the dendrite scale, with a prominent <100> crystallographic texture.
Conclusions:
- Epitaxial growth driven by the thermal gradient dictates the microstructure of SLM Inconel 718.
- The resulting microstructure exhibits significant <100> crystallographic texture and dendritic morphology.
- Detailed microstructural characterization is essential for optimizing heat treatments of additively manufactured Inconel 718.
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