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Related Concept Videos

X-ray Diffraction of Biological Samples01:10

X-ray Diffraction of Biological Samples

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X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal...
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X-ray Crystallography02:18

X-ray Crystallography

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The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
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Interference and Diffraction

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Interference is a characteristic phenomenon exhibited by waves. When two electromagnetic waves interact with their peaks and troughs coinciding, a resulting wave with enhanced amplitude is produced. This is known as constructive interference. In this case, the two waves interacting are in phase with each other.
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X-ray Imaging01:24

X-ray Imaging

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German physicist Wilhelm Röntgen (1845–1923) was experimenting with electrical current when he discovered that a mysterious and invisible "ray" would pass through his flesh but leave an outline of his bones on a screen coated with a metal compound. In 1895, Röntgen made the first durable record of the internal parts of a living human: an "X-ray" image (as it came to be called) of his wife’s hand. Scientists worldwide quickly began their own experiments with...
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Vapor Pressure02:34

Vapor Pressure

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When a liquid vaporizes in a closed container, gas molecules cannot escape. As these gas phase molecules move randomly about, they will occasionally collide with the surface of the condensed phase, and in some cases, these collisions will result in the molecules re-entering the condensed phase. The change from the gas phase to the liquid is called condensation. When the rate of condensation becomes equal to the rate of vaporization, neither the amount of the liquid nor the amount of the vapor...
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Gas pressure is caused by force exerted by gas molecules colliding with the surfaces of objects. Although the force of each collision is very small, any surface of an appreciable area experiences a large number of collisions in a short time, which can result in high pressure.
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Related Experiment Video

Updated: Jan 22, 2026

High Pressure Single Crystal Diffraction at PX^2
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X-ray magnetic diffraction under high pressure.

Yishu Wang1, T F Rosenbaum2, Yejun Feng3

  • 1The Institute for Quantum Matter and Department of Physics and Astronomy, The Johns Hopkins University, Baltimore, Maryland 21218, USA.

Iucrj
|July 19, 2019
PubMed
Summary
This summary is machine-generated.

X-ray magnetic diffraction techniques enable the study of spin and orbital behaviors in magnetic solids under extreme conditions. Researchers explored high-pressure, low-temperature magnetic transitions using advanced synchrotron methods.

Keywords:
X-ray magnetic diffractionantiferromagnetscryogenic temperatureshigh pressurenon-resonant X-ray diffraction of charge ordersresonant X-ray orbital scatteringspin-density-wave materials

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Area of Science:

  • Condensed Matter Physics
  • Materials Science
  • Magnetism

Background:

  • X-ray magnetic diffraction has advanced significantly since the 1980s.
  • It probes spin, orbital, and ionic degrees of freedom in magnetic solids.
  • Understanding their interplay is crucial for materials science.

Purpose of the Study:

  • To detail key challenges and methods for X-ray magnetic diffraction on single crystals.
  • To investigate high-pressure (above 40 GPa) and cryogenic (4 K) conditions.
  • To present case studies of magnetic transitions under pressure.

Main Methods:

  • Utilized non-resonant and resonant X-ray magnetic diffraction.
  • Employed diamond-anvil cell technology at third-generation synchrotron sources.
  • Studied single-crystal samples under high pressure and cryogenic temperatures.

Main Results:

  • Demonstrated X-ray magnetic diffraction capabilities for studying spin-flip transitions in incommensurate spin-density-wave materials.
  • Analyzed continuous quantum phase transitions in commensurate all-in-all-out antiferromagnets under pressure.
  • Showcased the athermal emergence and evolution of antiferromagnetism.

Conclusions:

  • These techniques are vital for exploring magnetic phenomena under extreme conditions.
  • Applicable to studying pressure evolution of charge order, orbital order, and charge superlattices.
  • Provides insights into the interplay between spin, charge, and lattice degrees of freedom.