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Benchtop High-MAS NMR for Paramagnetic Materials.

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Solid-state NMR backbone chemical shift assignments of α-synuclein amyloid fibrils at fast MAS regime.

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Related Experiment Video

Updated: Jan 21, 2026

Transport Properties of Ibuprofen Encapsulated in Cyclodextrin Nanosponge Hydrogels: A Proton HR-MAS NMR Spectroscopy Study
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H-MAS.

Ago Samoson1

  • 1Tallinn University of Technology, Estonia.

Journal of Magnetic Resonance (San Diego, Calif. : 1997)
|July 24, 2019
PubMed
Summary

New magic angle spinning (MAS) probes enable detailed structural and dynamics studies of large biomolecular structures. These probes offer high speeds and wide ranges for advanced solid-state nuclear magnetic resonance (ssNMR) experiments.

Area of Science:

  • Solid-state Nuclear Magnetic Resonance (ssNMR) spectroscopy
  • Biophysical chemistry
  • Materials science

Background:

  • Solid-state NMR is crucial for characterizing insoluble or non-crystalline biological macromolecules.
  • Traditional MAS probes have limitations in speed and acceleration, restricting the study of large and complex systems.
  • Advancements in probe technology are needed to expand the scope of ssNMR applications.

Purpose of the Study:

  • To introduce and characterize a novel generation of MAS probes.
  • To demonstrate the capabilities of these probes for 1H detection in solid and viscous samples.
  • To explore new experimental possibilities for studying large biomolecular structures.

Main Methods:

  • Characterization of a new MAS probe design.
Keywords:
MASStructural biology

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  • Testing probe performance at high rotational speeds (up to 170 kHz).
  • Evaluation of probe acceleration and speed range for diverse sample types.

    • Main Results:

    • The new MAS probes exhibit high top speeds (170 kHz) and a wide operational speed range.
    • Rapid acceleration allows for efficient data acquisition across various experimental conditions.
    • The probes facilitate detailed structural and dynamics studies of massive biomolecular assemblies.

    Conclusions:

    • This new generation of MAS probes significantly enhances the potential of ssNMR for investigating large biomolecular structures.
    • The improved performance opens avenues for novel ssNMR experiments previously not feasible.
    • These advancements contribute to a deeper understanding of the structure-dynamics-function relationship in complex biological systems.