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Fabricating High-viscosity Droplets using Microfluidic Capillary Device with Phase-inversion Co-flow Structure
Published on: April 17, 2018
Experimental study on factors affecting the end effect in gas viscosity measurement using capillary-tube viscometer
Xin Fang1, Xiang'an Yue1, Joseph Y Fu1
1State Key Laboratory of Petroleum Resources and Engineering, Key Laboratory of Petroleum Engineering Ministry of Education, China University of Petroleum, Beijing 102249, China.
This study introduces an improved capillary-tube viscometer to minimize end effect errors in viscosity measurements. By identifying threshold parameters, researchers developed an end-effect-free method for accurate gas viscosity determination.
Area of Science:
- Fluid Dynamics
- Physical Chemistry
- Metrology
Background:
- Capillary-tube viscometers are widely used for viscosity measurement due to their simplicity and adaptability.
- End effect corrections in capillary-tube viscometry introduce significant uncertainty in measurement results.
- Accurate viscosity measurement is crucial for various scientific and industrial applications, especially under high pressure.
Purpose of the Study:
- To investigate factors influencing the end effect in capillary-tube viscometry.
- To develop an end-effect-free method for accurate gas viscosity measurement.
- To improve the precision of capillary-tube viscometers, particularly for high-pressure applications.
Main Methods:
- Conducted high-pressure nitrogen viscosity measurements at low flow velocities using an improved capillary-tube viscometer.
- Analyzed the influence of flow velocity (v), tube inner diameter (d), and tube length (L) on the end effect.
- Defined a viscosity deviation coefficient (Ce) and identified threshold parameters (vthreshold, dthreshold, Lthreshold) for negligible end effect.
Main Results:
- The end effect's influence decreased with lower flow velocity and tube diameter, and inversely with tube length.
- Threshold parameters were identified where the viscosity deviation coefficient approached 1.0, indicating negligible end effect.
- The developed end-effect-free viscometry method achieved results with <1.2% error compared to NIST data for nitrogen viscosity.
Conclusions:
- Established an end-effect-free capillary-tube viscometry method applicable under specific experimental conditions.
- Demonstrated the method's accuracy and reliability by achieving good agreement with NIST standard data.
- Provided insights for enhancing the accuracy of capillary-tube viscometers in high-pressure gas viscosity measurements.
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