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Water-Mediated Synthesis of a Superionic Halide Solid Electrolyte.

Xiaona Li1, Jianwen Liang1, Ning Chen2

  • 1Department of Mechanical and Materials Engineering, University of Western Ontario, 1151 Richmond St, London, Ontario, N6A 3K7, Canada.

Angewandte Chemie (International Ed. in English)
|September 3, 2019
PubMed
Summary
This summary is machine-generated.

Researchers developed a new halide solid-state electrolyte (SSE), Li3InCl6, synthesized in water. This material exhibits high ionic conductivity and stability, advancing solid-state battery technology.

Keywords:
all-solid-state batteryaqueous synthesishalide solid electrolyteionic conductivitylithium

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Solid-State Batteries

Background:

  • Current solid-state electrolytes (SSEs) like polymers, oxides, and sulfides face limitations including high-temperature processing, air instability, and narrow electrochemical windows.
  • These limitations hinder the practical application of advanced solid-state batteries.
  • There is a critical need for SSEs with high ionic conductivity, air stability, wide electrochemical windows, and cost-effective mass production.

Purpose of the Study:

  • To develop a novel solid-state electrolyte (SSE) with improved properties for solid-state batteries.
  • To investigate a halide Li+ superionic conductor for its potential as a practical SSE.

Main Methods:

  • Synthesis of the halide Li+ superionic conductor, Li3InCl6, in an aqueous environment.
  • Measurement of ionic conductivity at room temperature (25°C).
  • Evaluation of the material's stability and recovery of ionic conductivity after water exposure.
  • Assembly and testing of a solid-state lithium battery using Li3InCl6 and a LiNi0.8Co0.1Mn0.1O2 cathode.

Main Results:

  • Li3InCl6 was successfully synthesized in water, demonstrating a low-cost and accessible production method.
  • The synthesized Li3InCl6 exhibited a high ionic conductivity of 2.04×10-3 S·cm-1 at 25°C.
  • The material demonstrated remarkable stability, with ionic conductivity recoverable even after dissolution in water.
  • The solid-state battery incorporating Li3InCl6 showed good cycling stability.

Conclusions:

  • Li3InCl6 is a promising halide superionic conductor for solid-state electrolytes.
  • Its synthesis in water and high ionic conductivity address key challenges in current SSE development.
  • The material's stability and performance in a solid-state battery suggest its potential for practical applications.