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Chenyao Hu1, Zupeng Chen2, Fengyan Han3

  • 1College of Chemical Engineering, Nanjing Forestry University, Nanjing, 210037, P. R. China.

Chemical Communications (Cambridge, England)
|October 26, 2019
PubMed

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Activated manganese(IV) oxide can selectively oxidize allylic and benzylic alcohols via a radical intermediate mechanism. Primary allylic alcohols are oxidized to aldehydes, while secondary allylic alcohols yield ketones. The redox reaction of potassium permanganate with an Mn(II) salt such as manganese sulfate (under either alkaline or acidic conditions), followed by thorough drying, yields the oxidizing agent: activated MnO2. While MnO2 is insoluble in the solvents used for the reaction, the...