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Improving EBSD precision by orientation refinement with full pattern matching.

A Winkelmann1,2, B M Jablon2,3, V S Tong3

  • 1Academic Centre for Materials and Nanotechnology, AGH University of Science and Technology, Krakow, Poland.

Journal of Microscopy
|January 31, 2020
PubMed
Summary
This summary is machine-generated.

High-precision orientation refinement using simulated pattern matching in electron backscatter diffraction (EBSD) offers superior accuracy for imaging microstructures. Postprocessing noisy EBSD data can reduce spatial resolution and introduce artifacts.

Keywords:
Electron backscatter diffractionKikuchi patternsorientation mappingscanning electron microscopy

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Area of Science:

  • Materials Science
  • Crystallography
  • Electron Microscopy

Background:

  • Electron Backscatter Diffraction (EBSD) is a key technique for crystallographic orientation mapping in scanning electron microscopy.
  • Conventional EBSD analysis relies on Hough-transform based methods, which may have limitations in precision.
  • Understanding and refining orientation data is crucial for characterizing microstructural features like dislocations and subgrains.

Purpose of the Study:

  • To compare the precision of different orientation imaging approaches using EBSD.
  • To evaluate the effectiveness of high-precision orientation refinement via simulated pattern matching.
  • To assess the impact of postprocessing filters on EBSD orientation data.

Main Methods:

  • Utilized EBSD for orientation imaging of WC grains.
  • Compared conventional Hough-transform EBSD with high-precision simulated pattern matching at full detector resolution (640 × 480 pixels).
  • Employed Electron Channeling Contrast Imaging (ECCI) for qualitative verification of orientation data.

Main Results:

  • Simulated pattern matching achieved a sensitivity of approximately 0.5 mrad (0.03°) and a spatial resolution of ~100 nm.
  • Postprocessing orientation data with filters can decrease spatial resolution.
  • Orientation filters may introduce artifacts, especially for features near the resolution limits of EBSD.

Conclusions:

  • High-precision orientation refinement using simulated pattern matching significantly enhances EBSD accuracy.
  • Careful consideration of postprocessing techniques is necessary to avoid loss of spatial resolution and artifact introduction in EBSD analysis.
  • The study provides insights into optimizing EBSD for detailed microstructural characterization.