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Updated: Dec 24, 2025

Preparation of Liquid-exfoliated Transition Metal Dichalcogenide Nanosheets with Controlled Size and Thickness: A State of the Art Protocol
Published on: December 20, 2016
Atomically thin PdSeO3 nanosheets: a promising 2D photocatalyst produced by quaternary ammonium intercalation and
Xiuming Zhang1, Jia Liu, Erhuang Zhang
1Beijing Key Laboratory of Construction Tailorable Advanced Functional Materials and Green Applications, Experimental Center of Advanced Materials, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China. liujia86@bit.edu.cn zhangjt@bit.edu.cn.
Abstract:
In 2018, the two-dimensional (2D) PdSeO3 monolayer was predicted to be a highly promising photocatalyst for direct overall water splitting in the light of density functional theory (DFT) computations. Herein, we present the first report on the synthesis of 2D PdSeO3 nanosheets by using the quaternary ammonium intercalation-assisted electrochemical exfoliation method. The resulting atomically thin PdSeO3 nanosheets possess a moderate band gap with suitable band edge alignments for water splitting, and display excellent activity and stability in photocatalytic H2 evolution.

