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Updated: Dec 23, 2025

Synthesis and Characterization of Amphiphilic Gold Nanoparticles
Published on: July 2, 2019
Surface Enhanced Raman Scattering (SERS) Effects of 4-Aminothiophenol on Au Nanoparticles with Different Shapes
Xiaochuan Xu1, Xiaofang Liu1, Min He1
1Key Laboratory of Synthetic and Natural Functional Molecule Chemistry (Ministry of Education), Shaanxi Key Laboratory of Physico-Inorganic Chemistry, College of Chemistry and Materials Science, Northwest University, Xi'an 710127, People's Republic of China.
Abstract:
Au nanoparticles with different shapes (nanosphere, nanoplate and nanorod) have been synthesized and were characterized by scanning electron microscope, transmission electron microscopy, X-ray diffraction and UV-vis absorption spectroscopy. We investigated the catalytic activity of Au nanoparticles with different morphologies as surface-enhanced Raman scattering substrates for the conversion of p-aminothiophenol to p,p'-dimercaptoazobenzene. The experimental results indicated that the order of catalytic activity is nanorod> nanoplate> nanosphere under 633 and 785 nm excitation. The current research provides some reliable insights and important references for exploration new catalysts and their catalytic activities from the perspectives of different sizes, morphology and crystal composition of nanomaterials.

