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Updated: Dec 22, 2025

Quantitative Atomic-Site Analysis of Functional Dopants/Point Defects in Crystalline Materials by Electron-Channeling-Enhanced Microanalysis
Published on: May 10, 2021
TEXS: in-vacuum tender X-ray emission spectrometer with 11 Johansson crystal analyzers
Mauro Rovezzi1, Alistair Harris2, Blanka Detlefs3
1Université Grenoble Alpes, CNRS, IRD, Irstea, Météo France, OSUG, FAME, 71 avenue des Martyrs, CS 40220, 38043 Grenoble, France.
Abstract:
The design and first results of a large-solid-angle X-ray emission spectrometer that is optimized for energies between 1.5 keV and 5.5 keV are presented. The spectrometer is based on an array of 11 cylindrically bent Johansson crystal analyzers arranged in a non-dispersive Rowland circle geometry. The smallest achievable energy bandwidth is smaller than the core hole lifetime broadening of the absorption edges in this energy range. Energy scanning is achieved using an innovative design, maintaining the Rowland circle conditions for all crystals with only four motor motions. The entire spectrometer is encased in a high-vacuum chamber that allocates a liquid helium cryostat and provides sufficient space for in situ cells and operando catalysis reactors.
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