Evaluation of Extrusion Temperatures, Pelleting Parameters, and Vitamin Forms on Vitamin Stability in Feed

Two experiments were conducted to determine the stability of microencapsulated and non-microencapsulated forms of vitamins in diets during extrusion and pelleting. We investigated the recovery of vitamins in swine diets after extrusion at 100 °C, 140 °C, or 180 °C. Next, two diets were conditioned at 65 °C (low temperature; LT) or 85 °C (high temperature; HT), and pellets were formed using a 2.5 × 15.0 mm (low length-to-diameter ratio; LR) or 2.5 × 20.0 mm (high length-to-diameter ratio; HR) die. The extrusion temperature had a significant effect on the recovery of vitamins E, B₁, B₂, B₃, and B₅ in the diets. The diet extruded at 100 °C had higher B₁, B₂, B₃, and B₅ vitamin recoveries than diets extruded at 140 °C and 180 °C. Microencapsulated vitamins A and K₃ had greater stability than non-microencapsulated vitamins A and K₃ at 100 °C and 140 °C extrusion. In the diet extruded at 180 °C, microencapsulated vitamins A, D₃, and K₃ had higher recoveries than non-microencapsulated vitamins A, D₃, and K₃. The recovery of vitamin K₃ in diets after LTLR (low temperature + low length-to-diameter ratio) or HTLR (high temperature + low length-to-diameter ratio) pelleting was greater (p < 0.05) than after LTHR (low temperature + high length-to-diameter ratio) and HTHR (high temperature + high length-to-diameter ratio) pelleting. Our results clearly show that low extrusion temperature and low pellet temperature, and a low length-to-diameter ratio (L:D ratio) for pellet mill die are recommended for pig feed. Moreover, microencapsulated vitamins had greater stability compared to non-microencapsulated vitamins.