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Published on: January 6, 2016
Preparation of boron nitrogen co-doped carbon quantum dots for rapid detection of Cr(VI)
Yueying Wang1, Xuetao Hu1, Wenting Li1
1Agricultural Product Processing and Storage Lab, School of Food and Biological Engineering, Jiangsu University, Zhenjiang, Jiangsu 212013, China; China-UK Joint Laboratory for Nondestructive Detection of Agro-products, Jiangsu University, Zhenjiang, Jiangsu 212013, China.
Abstract:
A novel fluorescent probe based on the static quenching and the inner filter effect between boron nitrogen co-doped carbon quantum dots (B, N-CDs) and Cr(VI) was developed for the quantitative determination of Cr(VI) in real water samples. B, N-CDs were prepared using the hydrothermal method with ammonium citrate and bis(pinacolato) diboron as raw materials. Compared with undoped CDs, the fluorescence properties of the B, N-CDs were improved. The fluorescence quantum yield of the B, N-CDs was as high as 59.01%. After optimization of the experimental parameters, the B, N-CDs could be used as a fluorescence probe to detect Cr(VI). Strong linear correlation (R2 = 0.9986) was established in the Cr(VI) concentration range 0.3-500 μM, and a detection limit of 0.24 μM was achieved. Moreover, the B, N-CDs successfully detected Cr(VI) in real water samples, indicating that they have broad application prospects in the sensitive detection of Cr(VI).
