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Electrospinning of PCL-Based Blends: Processing Optimization for Their Scalable Production.

Marina P Arrieta1,2, Adrián Leonés Gil1,3, Maysa Yusef1

  • 1Instituto de Ciencia y Tecnología de Polímeros (ICTP-CSIC), C/Juan de la Cierva 3, 28006 Madrid, Spain.

Materials (Basel, Switzerland)
|September 5, 2020
PubMed
Summary

This study optimized electrospinning for poly(ε-caprolactone) (PCL) mats blended with microcrystalline cellulose (MCC) or poly(3-hydroxybutyrate) (PHB). Blending with PHB significantly improved PCL fiber flexibility and mechanical properties for industrial use.

Keywords:
blendselectrospinningmicrocrystalline cellulosepoly(3-hydroxybutyrate)poly(ε-caprolactone)stretchability

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Area of Science:

  • Polymer Science
  • Materials Science
  • Biomaterials Engineering

Background:

  • Electrospun poly(ε-caprolactone) (PCL) mats are promising for industrial applications.
  • Optimizing processing parameters is crucial for scalable production.
  • Blending PCL with other polymers can enhance its properties.

Purpose of the Study:

  • To optimize electrospinning parameters for scalable PCL-based electrospun mats.
  • To investigate the effects of microcrystalline cellulose (MCC) and poly(3-hydroxybutyrate) (PHB) on PCL mat properties.
  • To characterize the morphological, thermal, and mechanical behavior of the developed blends.

Main Methods:

  • Optimization of electrospinning processing parameters.
  • Preparation of neat PCL, PCL-MCC, and PCL-PHB blends in various proportions.
  • Comprehensive characterization including Scanning Electron Microscopy (SEM), thermal analysis, and mechanical testing.

Main Results:

  • Addition of PHB reduced bead formation in electrospun PCL mats.
  • Both MCC and PHB decreased PCL's thermal stability but remained suitable for intended uses.
  • PCL-PHB blends showed increased stretchability (elongation at break up to 70%) and enhanced mechanical response compared to neat PCL.

Conclusions:

  • Scalable electrospun PCL mats can be produced by optimizing processing parameters.
  • Blending PCL with MCC or PHB allows for modulation of material properties.
  • PCL-PHB blends offer improved flexibility and mechanical strength, expanding their potential for industrial applications.