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Molding-type Solid-phase Extraction Media Glued with Commercially Available Adhesives.

Yuta Miki1, Hiroya Murakami2, Keisuke Iida1

  • 1Department of Applied Chemistry, Aichi Institute of Technology, 1247 Yachigusa, Yakusa-cho, Toyota, 470-0392, Japan.

Analytical Sciences : the International Journal of the Japan Society for Analytical Chemistry
|September 23, 2020
PubMed
Summary

A new molding-type solid-phase extraction medium (M-SPEM) overcomes particulate sorbent handling issues. This method uses adhesives to create M-SPEMs with high sorbent content and increased surface area for better extraction.

Keywords:
Solid-phase extraction mediacommercially available adhesiveglued sorbentmoldingparticulate sorbent

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Area of Science:

  • Analytical Chemistry
  • Materials Science

Background:

  • Particulate sorbents used in solid-phase extraction (SPE) present handling challenges due to static clinging and scattering.
  • Existing monolithic SPE media may not offer sufficient sorbent loading or surface area for optimal performance.

Purpose of the Study:

  • To develop a novel, simple production method for a molding-type solid-phase extraction medium (M-SPEM).
  • To improve the handling characteristics and performance of SPE media by increasing sorbent content and specific surface area.

Main Methods:

  • A production method for molding-type solid-phase extraction media (M-SPEM) was developed using commercially available adhesives.
  • The M-SPEM incorporates a high content of particulate sorbent, up to 85 wt%.

Main Results:

  • The developed M-SPEM effectively addresses the static clinging and scattering issues associated with particulate sorbents.
  • The high sorbent content in M-SPEM leads to a significantly higher specific surface area compared to previous monolithic media.
  • The M-SPEM facilitates easier and more efficient handling of sorbent materials.

Conclusions:

  • The simple molding-type solid-phase extraction medium (M-SPEM) offers a practical solution for overcoming handling difficulties with particulate sorbents.
  • The high sorbent loading and enhanced specific surface area of M-SPEMs suggest improved performance in solid-phase extraction applications.