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Updated: Nov 24, 2025
Author Spotlight: Development and Characterization of Eco-Friendly Lignin-Based Microparticles for Enhanced Delivery of Bioflavonoids
Published on: March 1, 2024
Facile synthesis of easily separated and reusable silver nanoparticles/aminated alkaline lignin composite and its
Yuxia Pang1, Zhengsong Chen1, Rubin Zhao1
1School of Chemistry and Chemical Engineering, Guangdong Engineering Research Center for Green Fine Chemicals, South China University of Technology, Guangzhou 510640, China.
Abstract:
Green synthesis of silver nanoparticles (AgNPs) has received increasing attention. In this study, AgNPs were prepared through in-situ reduction by aminated alkaline lignin (AAL). Compared with alkaline lignin (AL), AAL exhibited stronger reduction capacity (increased by 36%) due to the introduced amine groups and better water solubility. Moreover, the coordination effect of amine groups on AAL improved the binding force between lignin and AgNPs. The content of AgNPs in AgNPs/AAL composite were 2.4 times higher than that in AgNPs/AL, such content could be further increased through increasing the reduction pH or prolonging the heating time. The results of XPS, XRD and TEM showed that the AgNPs were spherical and monodisperse with an average particle size about 17 nm. Additionally, the size of AgNPs was affected by the amination degree of lignin. AgNPs/AAL exhibited good catalytic performance for the reduction of 4-nitrophenol to 4-aminophenol, and this compound could be easily recovered and reused for at least eight cycles.
