Application of the liquid-liquid dispersed microextraction based on phase transition behavior of temperature...

In this paper, temperature sensitive polymer p(MAH-β-CD-co-NIPAM) was used as extraction in DLLME, because its phase transition behavior can be observed at room temperature due to Hofmeister and non-co-solvent effect. The whole pretreatment process is simple and fast, and the extraction process did not require dispersant to assist dispersion and centrifugation to collect the adsorbent. A new analytical method based on DLLME coupled with HPLC-UV was developed to detect five types of BPs in milk and take-out packaging. The limits of detection ranged from 0.44 to 1.60 ng mL^-1 (S/N = 3). The relative recoveries of 5 BPs in food packaging were in the range of 91.08-108.04%.