Related Experiment Video
Updated: Oct 27, 2025

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Peculiarities of DRX in a Highly-Alloyed Austenitic Stainless Steel
Pavel Dolzhenko1, Marina Tikhonova1, Rustam Kaibyshev1
1Laboratory of Mechanical Properties of Nanostructured Materials and Superalloys, Belgorod State University, 308015 Belgorod, Russia.
Abstract:
The features of discontinuous dynamic recrystallization (DRX) in a highly-alloyed austenitic stainless steel were studied at temperatures of 800 °C to 1100 °C. Hot deformation accompanied by DRX was characterized by an activation energy of 415 kJ/mol. The frequency of the sequential DRX cycles depended on the deformation conditions; and the largest fraction of DRX grains with small grain orientation spread below 1° was observed at a temperature of around 1000 °C and a strain rate of about 10-3 s-1. The following power law relationships were obtained for DRX grain size (DDRX) and dislocation density (ρ) vs. temperature-compensated strain rate (Z) or peak flow stress (σP): DDRX ~ Z-0.25, ρ ~ Z0.1, σP ~ DDRX-0.9, σP ~ ρ1.4. The latter, i.e., σP ~ ρ1.4, was valid in the flow stress range below 300 MPa and changed to σP ~ ρ0.5 on increasing the stress. The obtained dependencies suggest a unique power law function between the dislocation density and the DRX grain size with an exponent of -0.5.
More Related Videos
12:18Co-localizing Kelvin Probe Force Microscopy with Other Microscopies and Spectroscopies: Selected Applications in Corrosion Characterization of Alloys
Published on: June 27, 2022
08:55Methods of Ex Situ and In Situ Investigations of Structural Transformations: The Case of Crystallization of Metallic Glasses
Published on: June 7, 2018
Related Concept Videos
X-ray Diffraction of Biological Samples
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are scattered by the electron clouds around the sample atoms. The X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal...
Mechanical Characteristics of Steel
The tension test is fundamental for determining tensile strength. In this test, a steel specimen is stretched using a gripping device until it breaks. The data collected during this test are used...
X-ray Crystallography
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
Stress-Strain Diagram - Ductile Materials