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Updated: Oct 25, 2025

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy
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Quantitative rotational-echo double resonance for Carbon-13 spin clusters

Shigeru Matsuoka1, Miriam Sindelar2, Sonal Bansal2

  • 1Department of Chemistry, Washington University, St. Louis, MO 63130, USA; Faculty of Medicine, Oita University, Oita 879-5593, Japan.

Journal of Magnetic Resonance (San Diego, Calif. : 1997)
|August 7, 2021
PubMed
Summary

Rotational-echo double resonance (REDOR) for clusters of 13C spins (RDX) achieves quantitative analysis of 13C clusters. This method, RDX24, enables precise characterization of nitrogen isotopic enrichments in cellular proteins.

Keywords:
(13)C spin clusters(15)N distributionsHuman embryonic kidney cellsRecouplingSolid state NMR

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