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Scanning SQUID microscopy in a cryogen-free dilution refrigerator.
D Low1, G M Ferguson1, Alexander Jarjour1
1Laboratory of Atomic and Solid-State Physics, Cornell University, Ithaca, New York 14853, USA.
The Review of Scientific Instruments
|September 2, 2021
Summary
We developed a scanning superconducting quantum interference device (SQUID) microscope operating at 30 mK in a cryogen-free system. This allows for high-resolution magnetic imaging of micro-scale devices.
Area of Science:
- Condensed Matter Physics
- Quantum Sensing
- Cryogenic Engineering
Background:
- Superconducting Quantum Interference Devices (SQUIDs) are highly sensitive magnetometers.
- Achieving millikelvin temperatures is crucial for studying quantum phenomena.
- Cryogen-free systems offer advantages in accessibility and operational simplicity.
Purpose of the Study:
- To develop and demonstrate a scanning SQUID microscope capable of operation at millikelvin temperatures in a cryogen-free environment.
- To achieve micrometer-scale magnetic imaging resolution.
- To enable simultaneous measurement of static magnetic fields, magnetic susceptibility, and current-induced magnetic fields.
Main Methods:
- Integration of a scanning SQUID microscope into a cryogen-free dilution refrigerator.
- Rigid mounting of the microscope to the mixing chamber for optimal thermal anchoring.
- Implementation of vibration isolation techniques and a rigid microscope housing.
- Operation within a superconducting vector magnet.
- Simultaneous acquisition of multiple magnetic field signals.
Main Results:
- Successful operation of the SQUID microscope at a base temperature of at least 30 mK.
- Achieved micrometer resolution imaging over a 150 µm range with stable base temperature.
- Demonstrated simultaneous imaging of static magnetic fields, magnetic susceptibility, and current-induced fields.
- Minimized relative vibrations between the SQUID sensor and the sample.
Conclusions:
- The developed cryogen-free scanning SQUID microscope provides a versatile platform for high-resolution magnetic imaging at millikelvin temperatures.
- The system enables detailed characterization of superconducting devices and quantum materials.
- This technology advances the study of nanoscale magnetic phenomena in accessible cryogenic conditions.

