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Updated: Oct 11, 2025

Quantitative Atomic-Site Analysis of Functional Dopants/Point Defects in Crystalline Materials by Electron-Channeling-Enhanced Microanalysis
Published on: May 10, 2021
Multi-scale analyses of constituent phases in a trip-assisted duplex stainless steel by electron backscatter
Wanchuck Woo1, Jongyul Kim1, Eun-Young Kim2
1Neutron Science Center, Korea Atomic Energy Research Institute, Daejeon 34057, South Korea.
Abstract:
Micrometer to centimeter scale analyses of the crystalline phase volume fractions in a trip-assisted duplex stainless steel were performed under loading using electron backscatter diffraction (EBSD), in situ neutron diffraction, and energy selective neutron imaging (ESNI) methods. In contrast to the localized investigations of EBSD, ESNI provides macroscopic spatial distributions in a volume-averaged manner over the entire specimen with a spatial resolution of about 65 microm. The ESNI shows that the martensite is concentrated on the necking region and estimates its volume fraction of 14% at a strain of 0.2, which is comparable to the neutron diffraction result.
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