Integrative geochronology calibrates the Middle and Late Stone Ages of Ethiopia's Afar Rift

The Halibee member of the Upper Dawaitoli Formation of Ethiopia's Middle Awash study area features a wealth of Middle and Later Stone Age (MSA and LSA) paleoanthropological resources in a succession of Pleistocene sediments. We introduce these artifacts and fossils, and determine their chronostratigraphic placement via a combination of established radioisotopic methods and a recently developed dating method applied to ostrich eggshell (OES). We apply the recently developed ²³⁰Th/U burial dating of OES to bridge the temporal gap between radiocarbon (¹⁴C) and ⁴⁰Ar/³⁹Ar ages for the MSA and provide ¹⁴C ages to constrain the younger LSA archaeology and fauna to ∼24 to 21.4 ka. Paired ¹⁴C and ²³⁰Th/U burial ages of OES agree at ∼31 ka for an older LSA locality, validating the newer method, and in turn supporting its application to stratigraphically underlying MSA occurrences previously constrained only by a maximum ⁴⁰Ar/³⁹Ar age. Associated fauna, flora, and Homo sapiens fossils are thereby now fixed between 106 ± 20 ka and 96.4 ± 1.6 ka (all errors 2σ). Additional ⁴⁰Ar/³⁹ results on an underlying tuff refine its age to 158.1 ± 11.0 ka, providing a more precise minimum age for MSA lithic artifacts, fauna, and H. sapiens fossils recovered ∼9 m below it. These results demonstrate how chronological control can be obtained in tectonically active and stratigraphically complex settings to precisely calibrate crucial evidence of technological, environmental, and evolutionary changes during the African Middle and Late Pleistocene.