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Updated: Oct 3, 2025

Sample Preparation and Experimental Design for In Situ Multi-Beam Transmission Electron Microscopy Irradiation Experiments
Published on: June 27, 2022
Irradiation of W and K-Doped W Laminates without or with Cu, V, Ti Interlayers under a Pulsed 6 MeV Electron Beam
D Ticoș1, M Galaţanu2, A Galaţanu2
1National Institute for Laser, Plasma and Radiation Physics, Atomistilor Street 409, Magurele, 077125 Ilfov, Romania.
Abstract:
Small multilayered laminated samples consisting of stacks of W (or K-doped W) foils without an interlayer or with interlayers from Cu, V, and Ti were exposed to a pulsed electron beam with an energy of 6 MeV in several irradiation sessions. All samples maintained their macroscopic integrity, suggesting that the W-metal laminate concept is compatible with high heat flux applications. The surface of the samples was analyzed using a scanning electron microscope (SEM) before and after each irradiation session. The experimental results indicate that electron beam irradiation induces obvious modifications on the surface of the samples. Morphological changes such as the appearance of nanodroplets, nanostructures, and melting and cracking, depending on the sample type and the electron beam fluence, are observed. The irradiation is carried out in a vacuum at a pressure of 2 to 4 × 10-2 torr, without active cooling for the samples. The structures observed on the surface of the samples are likely due to electron beam heating and vaporization followed by vapor condensation in the volume adjacent to the surface.
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