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Millisecond timescale reactions observed via X-ray spectroscopy in a 3D microfabricated fused silica mixer.

Diego A Huyke1, Ashwin Ramachandran1, Oscar Ramirez-Neri2

  • 1Stanford University, Stanford, CA 94305, USA.

Journal of Synchrotron Radiation
|May 5, 2022
PubMed

Keywords:
3D microfabricationX-ray spectroscopykineticsmicrofluidicsmixing

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Fast reactions occurring in times shorter than the time needed to mix reactants pose a unique challenge for investigation. In a liquid-phase continuous-flow system, reactants A and B are swiftly pushed into the mixing chamber, where mixing occurs within 1 ms. The reaction mixture then flows through an observation tube, and one measures light absorption to determine species concentrations at various points of the tube. This method is most appropriate when relatively large volumes of reactants...