Test Methods for Characterizing the Properties of Fiber-Reinforced Polymer Composites at Elevated Temperatures

Recent research trends focus on developing bio-based (derived from agricultural byproducts) fiber-reinforced polymer (FRP) composites for structural applications. Fire resistance is one of the key issues that need to be addressed for the use of these FRP materials in buildings. The thermal and mechanical properties of the constituent materials essentially determine the fire performance (and the fire resistance rating) of a structural member, and these properties vary with temperature. Further, the properties of composite materials such as the FRP are highly influenced by the composition and type of fibers and matrix, and these thermo-mechanical properties also vary significantly with temperature. Due to this variation, the fire resistance of FRP materials (both conventional and bio-based) poses a major concern for use in buildings. Currently, very few standardized test procedures are available for evaluating the high-temperature material properties of FRP composites. In this paper, a review of testing protocols and procedures for undertaking tests on FRP materials at various elevated temperatures for evaluating their properties is carried out. Recommendations are provided on the most suitable test methods, specimen conditions, testing regime, and other issues associated with testing at elevated temperatures. In addition, the applicability of the proposed test methods is illustrated through a case study on conventional FRP specimens. Further, the applicability of the recommended test procedures for measuring high-temperature properties of bio-based FRP composites is highlighted.