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Updated: Jul 18, 2026
Three-Dimensionally Printed Microfluidic Cross-flow System for Ultrafiltration/Nanofiltration Membrane Performance Testing
Published on: February 13, 2016
Preparation and Characterization of Modified Polysulfone with Crosslinked Chitosan-Glutaraldehyde MWCNT
Ahmed A Alshahrani1, Abeer A El-Habeeb2, Noor H Alotaibi2
1Nuclear Science Research Institute, King Abdul Aziz City for Science and Technology, P.O. Box 6086, Riyadh 11442, Saudi Arabia.
Abstract:
Nanofiltration membranes were successfully created using multi-walled carbon nanotubes (MWCNTs) and MWCNTs modified with amine (MWCNT-NH2) and carboxylic groups (MWCNT-COOH). Chitosan (CHIT) and chitosan−glutaraldehyde (CHIT-G) were utilized as dispersants. Sonication, SEM, and contact angle were used to characterize the as-prepared membranes. The results revealed that the type of multi-walled carbon nanotubes (MWCNT, MWCNT-COOH and MWCNT-NH2) used as the top layer had a significant impact on membrane characteristics. The lowest contact angle was 38.6 ± 8.5 for the chitosan-G/MWCNT-COOH membrane. The surface morphology of membranes changed when carbon with carboxylic or amine groups was introduced. In addition, water permeability was greater for CHIT-G/MWCNT-COOH and CHIT-G/MWCNT-NH2 membranes. The CHIT-G/MWCNT-COOH membrane had the highest water permeability (5.64 ± 0.27 L m−2 h−1 bar−1). The findings also revealed that for all membranes, the rejection of inorganic salts was in the order R(NaCl) > R(MgSO4).
