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In Situ Characterization of Boehmite Particles in Water Using Liquid SEM
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In Situ Inclusion Detection and Material Characterization in an Electron Beam Powder Bed Fusion Process Using

Martin Gardfjell1, Marcel Reith1, Martin Franke1

  • 1Neue Materialien Fürth GmbH, 90762 Fürth, Germany.

Materials (Basel, Switzerland)
|June 28, 2023
PubMed
Summary

Electron Optical Imaging (ELO) in Electron Beam Powder Bed Fusion (PBF-EB) can detect 100 μm foreign powder particles. ELO also accurately predicts alloy effective atomic number (Zeff) for material characterization.

Keywords:
Additive ManufacturingBackscattered Electron DetectionElectron Beam Powder Bed FusionElectron Optical ImagingInclusion DetectionPowder ContaminationProcess Monitoring

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Area of Science:

  • Additive Manufacturing
  • Materials Science
  • Process Monitoring

Background:

  • Electron Beam Powder Bed Fusion (PBF-EB) uses an electron beam to melt metal powder.
  • Electron Optical Imaging (ELO) leverages backscattered electrons for process monitoring.
  • ELO's material contrast capabilities for PBF-EB are not well-understood.

Purpose of the Study:

  • Investigate the extent of material contrast using ELO in PBF-EB.
  • Assess ELO's ability to detect powder contamination.
  • Explore ELO for material characterization via effective atomic number (Zeff) prediction.

Main Methods:

  • Utilized ELO with a backscattered electron detector during PBF-EB.
  • Focused on identifying foreign powder particles based on backscattering coefficients.
  • Developed a mathematical model linking ELO signal intensity to Zeff.

Main Results:

  • Demonstrated ELO's capability to distinguish 100 μm foreign particles with higher backscattering coefficients.
  • Successfully predicted the effective atomic number (Zeff) of alloys within ±1 atomic number.
  • Verified the model with empirical data from twelve distinct materials.

Conclusions:

  • ELO is effective for detecting small foreign particles in PBF-EB.
  • ELO provides a viable method for non-destructive material characterization in PBF-EB.
  • The developed framework accurately relates ELO signal intensity to alloy Zeff.