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Updated: Jul 15, 2025

Determining the Mechanical Strength of Ultra-Fine-Grained Metals
Published on: November 22, 2021
Determining Stress in Metallic Conducting Layers of Microelectronics Devices Using High Resolution Electron
Timothy Ruggles1, Scott Grutzik1, Kelly Stephens1
1Sandia National Laboratories, 1515 Eubank SE, Albuquerque, NM 87123, USA.
Delayed failure in microelectronics from stress voiding can be predicted. A new method uses substrate distortions measured by high-resolution electron backscatter diffraction (HREBSD) to determine internal stresses in metallic layers.
Area of Science:
- Materials Science
- Microelectronics Reliability
- Solid Mechanics
Background:
- Aging microelectronics face delayed failure due to stress voiding, where voids can cause open circuits.
- Accurate stress measurement in metallic layers is vital for predicting this failure mode.
- Direct stress measurement is challenging as exposing conductive lines relieves stress.
Purpose of the Study:
- To develop and validate a novel technique for measuring internal stresses in microelectronic metallic layers.
- To investigate stress distribution in legacy microelectronic components, with and without visible voids.
- To provide a method for comparing experimental stress data with theoretical stress voiding models.
Main Methods:
- Mechanical thinning of the device substrate to access internal layers.
- High-resolution electron backscatter diffraction (HREBSD) to measure surface distortions on the thinned substrate.
- Finite element analysis (FEA) to correlate substrate distortions with subsurface stresses in metallic layers.
Main Results:
- Stresses in legacy components without apparent voids were found to be approximately 300 MPa, matching theoretical manufacturing stresses.
- Distortion fields around known voids were successfully mapped, providing data for direct comparison with stress voiding models.
- The HREBSD technique, combined with FEA, effectively infers subsurface stresses in layered microelectronic devices.
Conclusions:
- The presented HREBSD coupled with FEA is a valuable non-destructive technique for assessing stress and predicting failure in microelectronics.
- This method allows for the characterization of stress states in aging components, crucial for reliability assessments.
- The ability to map distortion fields around voids offers new avenues for validating and refining stress voiding failure models.
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