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A Two-Step Approach to Orange Peel Waste Valorization: Consecutive Extraction of Pectin and Hesperidin
Onofre Figueira1, Verónica Pereira1, Paula C Castilho1
1CQM-Centro de Química da Madeira, Campus da Penteada, Universidade da Madeira, 9200-105 Funchal, Portugal.
Foods (Basel, Switzerland)
|October 28, 2023
Summary
This study presents a green chemistry approach to extract pectin and hesperidin from orange peel waste. The novel consecutive extraction method maximizes citrus residue potential for valuable food industry compounds.
Area of Science:
- Food Science
- Green Chemistry
- Biotechnology
Background:
- Citrus waste presents disposal challenges and environmental concerns.
- Current single-compound extraction methods underutilize citrus residue potential.
- Optimizing extraction schemes is crucial for maximizing bioactive compound recovery.
Purpose of the Study:
- To design a consecutive extraction process for pectin and hesperidin from orange peel waste.
- To develop an eco-friendly method for hesperidin extraction and precipitation.
- To assess the potential of citrus waste as a source of high-value food ingredients.
Main Methods:
- Neutral pretreatment followed by acidic pectin extraction.
- Consecutive hesperidin extraction utilizing a drastic pH change.
- Optimization of hesperidin extraction conditions (time, temperature, solvent ratio).
Main Results:
- Pectin with high AUA content (66.20 ± 1.25%) suitable for the food industry was obtained.
- Optimal hesperidin extraction (30 min, 70 °C, 1:10 w/v) yielded 1% with 84% purity.
- The consecutive extraction scheme demonstrated feasibility and efficiency.
Conclusions:
- Citrus waste can be valorized into high-quality pectin and hesperidin.
- The developed method aligns with green chemistry and circular economy principles.
- This approach offers significant potential for the food industry.

