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Updated: Jul 9, 2025

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
Published on: June 19, 2018
An innovative in situ AFM system for a soft X-ray spectromicroscopy synchrotron beamline
Aljoša Hafner1, Luca Costa2, George Kourousias1
1Elettra Sincrotrone Trieste, SS 14 km 163, 5 in Area Science Park, 34149 Basovizza, Trieste, Italy. alessandra.gianoncelli@elettra.eu.
Abstract:
Multimodal imaging and spectroscopy like concurrent scanning transmission X-ray microscopy (STXM) and X-ray fluorescence (XRF) are highly desirable as they allow retrieving complementary information. This paper reports on the design, development, integration and field testing of a novel in situ atomic force microscopy (AFM) instrument for operation under high vacuum in a synchrotron soft X-ray microscopy STXM-XRF end-station. A combination of μXRF and AFM is demonstrated for the first time in the soft X-ray regime, with an outlook for the full XRF-STXM-AFM combination.
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