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Related Concept Videos

High-Performance Liquid Chromatography: Types of Detectors01:15

High-Performance Liquid Chromatography: Types of Detectors

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The role of the detectors in High-Performance Liquid Chromatography (HPLC) is to analyze the solutes as they exit from the chromatographic column. The detector recognizes the solute's property and generates corresponding electrical signals, which are converted into a readable graph of the detector's response versus elution time called a chromatogram at the computer. There are several types of HPLC detectors, each with its own advantages and limitations, depending on the analyte...
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Optrode-Assisted Multiparametric Near-Infrared Spectroscopy for the Analysis of Liquids.

Maria Giulia Delli Santi1, Salvatore Castrignano1, Marialuisa Capezzuto1

  • 1Consiglio Nazionale delle Ricerche, Istituto Nazionale di Ottica (CNR-INO), Via Campi Flegrei 34, 80078 Pozzuoli, Italy.

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This study presents a novel optical fiber sensor system for simultaneous, multiparametric analysis of liquid samples. The compact, integrated setup enables real-time spectral and refractive index measurements.

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NIR spectroscopyfiber optics sensorslab-on-fiber sensorsmultiparametric analysisportable spectrometers

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Area of Science:

  • Optoelectronics
  • Spectroscopy
  • Chemical Sensing

Background:

  • Multiparametric analysis of liquid samples is crucial for various applications.
  • Existing methods often require complex and bulky setups.
  • Integrating multiple optical fiber sensors offers a potential solution for miniaturization.

Purpose of the Study:

  • To develop a compact sensing scheme for simultaneous multiparametric analysis of liquid analytes.
  • To integrate multiple optical fiber sensors within a near-infrared spectrometer.
  • To validate the proposed method for real-time spectral and refractive index measurements.

Main Methods:

  • A broadband radiation source is encoded into a time-domain interferogram.
  • The encoded signal is distributed to multiple sensing units for simultaneous sample interrogation.
  • Spectral readout is achieved using Fourier transform routines on output signals.
  • A plasmonic nanostructured fiber probe and transmission cuvette were employed for validation.

Main Results:

  • Demonstrated simultaneous measurement of absorption spectrum and refractive index.
  • Successfully performed multiparametric analysis of water-methanol solutions.
  • Validated the integration of sensing units within a robust telecom optical fiber.

Conclusions:

  • The proposed optofluidic method enables compact and simultaneous multiparametric analysis of liquid samples.
  • The integrated optical fiber sensor system offers a robust and versatile platform for chemical sensing.
  • This approach simplifies complex spectral and refractive index measurements.