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Atomic Emission Spectroscopy: Instrumentation01:22

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The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
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A solid-state high harmonic generation spectrometer with cryogenic cooling.

Finn Kohrell1,2, Bailey R Nebgen2,3, Jacob A Spies2,3

  • 1Institute for Optics and Quantum Electronics, Friedrich Schiller University Jena, 07743 Jena, Germany.

The Review of Scientific Instruments
|February 28, 2024
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Summary
This summary is machine-generated.

We developed an advanced solid-state high harmonic generation (sHHG) spectrometer for cryogenic measurements. This new tool enables temperature-dependent sHHG studies of condensed matter, especially highly correlated materials at low temperatures.

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Area of Science:

  • Condensed matter physics
  • Quantum optics
  • Spectroscopy

Background:

  • Solid-state high harmonic generation (sHHG) spectroscopy is a powerful method for probing electronic properties.
  • Current limitations hinder low-temperature measurements, restricting studies of emergent quantum phenomena.

Purpose of the Study:

  • To implement an advanced sHHG spectrometer capable of cryogenic temperature measurements.
  • To enable temperature-dependent sHHG spectroscopy down to a few Kelvin.

Main Methods:

  • Construction of a sHHG spectrometer within a vacuum chamber and closed-cycle helium cryostat.
  • Integration of an in situ temperature probe to monitor sample temperature.
  • Application of high-intensity femtosecond laser pulses for harmonic generation.

Main Results:

  • The spectrometer successfully maintained cryogenic temperatures in the sample interaction region during laser excitation.
  • Demonstrated the capability for temperature-dependent sHHG measurements at cryogenic levels.

Conclusions:

  • The developed cryogenic sHHG spectrometer is a novel tool for low-temperature condensed matter research.
  • This technique is particularly valuable for investigating highly correlated materials and their low-temperature emergent phases.