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Related Concept Videos

X-ray Crystallography02:18

X-ray Crystallography

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The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
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Heteronuclear correlation spectroscopy is an analytical technique that investigates the coupling between different types of nuclei, often a proton and an X-nucleus, such as carbon-13 or nitrogen-15. This method is commonly used in nuclear magnetic resonance (NMR) spectroscopy to gain insights into complex chemical compounds' structural and compositional aspects. A typical heteronuclear correlation spectrum displays X-nucleus chemical shifts on one axis and a proton spectrum on the other...
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High-pressure X-ray photon correlation spectroscopy at fourth-generation synchrotron sources.

Antoine Cornet1, Alberto Ronca1, Jie Shen1

  • 1Institut Néel, Université Grenoble Alpes and Centre National de la Recherche Scientifique, 25 rue des Martyrs - BP 166, 38042 Grenoble, France.

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A new setup enables X-ray photon correlation spectroscopy (XPCS) under extreme pressures (multi-gigapascals) and temperatures. This technique probes atomic-scale dynamics in complex materials, advancing condensed matter physics research.

Keywords:
X-ray photon correlation spectroscopycomplex systemsfourth-generation synchrotron sourceshigh-pressure XPCShigh-pressure sample environmentsmetallic glassessupercooled liquid states

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Area of Science:

  • Condensed Matter Physics
  • Materials Science
  • Spectroscopy

Background:

  • Studying atomic-scale dynamics in complex systems under extreme conditions is crucial for understanding material properties.
  • Traditional methods face limitations in achieving multi-gigapascal pressures and high temperatures while maintaining measurement sensitivity.

Purpose of the Study:

  • To develop and validate a novel experimental setup for high-pressure X-ray photon correlation spectroscopy (XPCS).
  • To enable in-situ monitoring of internal material motion at the atomic scale under pressures up to the multi-gigapascal range and temperatures up to 600 K.

Main Methods:

  • Combining hard X-ray XPCS with a specialized high-pressure sample environment.
  • Utilizing high-flux coherent X-rays from fourth-generation synchrotrons to overcome diamond anvil cell absorption.
  • Measuring the intermediate scattering function over six orders of magnitude in time (10⁻³ s to 10³ s).

Main Results:

  • Demonstrated the feasibility of performing XPCS experiments in the multi-gigapascal pressure range.
  • Successfully measured pressure-dependent dynamics in metallic glasses.
  • Addressed challenges related to X-ray coherence, sample stability, and pressure/temperature control.

Conclusions:

  • The developed high-pressure XPCS technique is a powerful tool for investigating the behavior of complex systems under extreme conditions.
  • This advancement opens new avenues for exploring pressure-induced phase transitions and dynamics in materials science.
  • Future research can leverage this setup to uncover fundamental insights into material properties at the atomic scale.