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Updated: Aug 8, 2026
Reductive Electropolymerization of a Vinyl-containing Poly-pyridyl Complex on Glassy Carbon and Fluorine-doped Tin Oxide Electrodes
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Fabrication of polycrystalline phosphorus-doped diamond electrodes from red phosphorus
Tomokiyo Moriguchi1,2, Mai Tomisaki3, Susumu Sato4
1Department of Chemistry, Keio University, 3-14-1 Hiyoshi, Yokohama 223-8522, Japan. einaga@chem.keio.ac.jp.
Abstract:
Polycrystalline phosphorus-doped diamond was fabricated by the quartz-tube-type microwave plasma-assisted chemical vapor deposition method. Significantly, red phosphorus was used as a source of phosphorous, instead of PH3. Phosphorus-doped diamond electrodes with hydrogen-terminated and oxygen-terminated surfaces were investigated for the redox reactions of K3[Fe(CN)6] and [Ru(NH3)6]Cl3. The carrier concentration was estimated as 2.1-5.3 × 1018 cm-3 from electrochemical impedance measurements. Polycrystalline phosphorus-doped diamond shows great promise as chemical electrode materials.
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