Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Video

Updated: Jun 22, 2025

Synthesis and Reaction Chemistry of Nanosize Monosodium Titanate
08:44

Synthesis and Reaction Chemistry of Nanosize Monosodium Titanate

Published on: February 23, 2016

8.6K

A Metatitanic Acid Particulate Xerogel: Green Synthesis, Structure Determination, and Detailed Characterization.

Monika Motlochová1,2, Xenia Vislocká1, Sven Lidin2

  • 1Institute of Inorganic Chemistry of the Czech Academy of Sciences, 250 68 Řež, Czech Republic.

Inorganic Chemistry
|June 29, 2024
PubMed
Summary

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Advanced Biomaterials in Tissue Engineering Based on Antibacterial and Antibiofilm Nanocomposites for Multidrug-Resistant Wound Pathogens.

ACS omega·2026
Same author

Vacancy-Mediated NiAs-Ni<sub>2</sub>In-Type Intermetallic Phases: Ni<sub>1+δ</sub>(In/Sb).

Inorganic chemistry·2026
Same author

Novel core-shell Fe<sub>3</sub>O<sub>4</sub>/NiO nanofibers for the photocatalytic degradation of active pharmaceutical compounds.

RSC advances·2025
Same author

Comparison of Cytotoxicity and Photocatalytic Properties of Iron Vanadate Nanoparticles with Commercial Catalysts: For the Degradation of Microplastics and Bacterial Inactivation Application.

ACS omega·2025
Same author

Novel Core-Shell Metal Oxide Nanofibers with Advanced Optical and Magnetic Properties Deposited by Co-Axial Electrospinning.

Nanomaterials (Basel, Switzerland)·2025
Same author

Iron <i>N</i>-Heterocyclic Carbene Photoactive Complexes with Rigid Phenylethynyl Substituents as Ligand π-System Extensions.

Inorganic chemistry·2025

This study introduces an eco-friendly method for preparing metatitanic acid using titanyl sulfate and sodium hydroxide. The process preserves precursor morphology and yields nanoporous metatitanic acid with high surface area.

Area of Science:

  • Materials Science
  • Inorganic Chemistry
  • Nanotechnology

Background:

  • Metatitanic acid is a crucial titanium compound.
  • Existing preparation methods may involve hazardous substances or alter material properties.
  • There is a need for controlled synthesis of metatitanic acid with specific characteristics.

Purpose of the Study:

  • To develop an environmentally safe synthesis route for metatitanic acid.
  • To investigate the preparation of metatitanic acid with preserved morphology and tunable parameters.
  • To characterize the structural and physical properties of the synthesized metatitanic acid.

Main Methods:

  • Reaction of solid titanyl sulfate with aqueous sodium hydroxide.
  • Controlled variation of the alkali metal/titanyl sulfate ratio.

More Related Videos

Chemical Synthesis of Porous Barium Titanate Thin Film and Thermal Stabilization of Ferroelectric Phase by Porosity-Induced Strain
08:00

Chemical Synthesis of Porous Barium Titanate Thin Film and Thermal Stabilization of Ferroelectric Phase by Porosity-Induced Strain

Published on: March 27, 2018

11.1K
Synthesis of Zeolites Using the ADOR Assembly-Disassembly-Organization-Reassembly Route
08:26

Synthesis of Zeolites Using the ADOR Assembly-Disassembly-Organization-Reassembly Route

Published on: April 3, 2016

13.3K

Related Experiment Videos

Last Updated: Jun 22, 2025

Synthesis and Reaction Chemistry of Nanosize Monosodium Titanate
08:44

Synthesis and Reaction Chemistry of Nanosize Monosodium Titanate

Published on: February 23, 2016

8.6K
Chemical Synthesis of Porous Barium Titanate Thin Film and Thermal Stabilization of Ferroelectric Phase by Porosity-Induced Strain
08:00

Chemical Synthesis of Porous Barium Titanate Thin Film and Thermal Stabilization of Ferroelectric Phase by Porosity-Induced Strain

Published on: March 27, 2018

11.1K
Synthesis of Zeolites Using the ADOR Assembly-Disassembly-Organization-Reassembly Route
08:26

Synthesis of Zeolites Using the ADOR Assembly-Disassembly-Organization-Reassembly Route

Published on: April 3, 2016

13.3K
  • Characterization using chemical analysis, structural analysis, electron microscopy, and local analysis.

    • Main Results:

    • Successful synthesis of metatitanic acid using only environmentally safe precursors.
    • Preservation of the starting titanyl sulfate morphology in the final product.
    • Formation of pseudomorphic aggregates with regular nanoporosity (up to 500 m²/g), high mechanical resistance, and no tendency to form colloids.
    • Production of metatitanic acid with tunable alkali metal and sulfate anion content.
    • Identification of very small (2-3 nm) weakly crystalline particles within the aggregates.

    Conclusions:

    • The developed method offers a sustainable and controlled approach to metatitanic acid preparation.
    • The resulting metatitanic acid exhibits unique structural and physical properties suitable for various applications.
    • The study provides insights into the formation mechanism and the structure of metatitanic acid.