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Updated: May 15, 2025

Quantitative 31P NMR Analysis of Lignins and Tannins
Published on: August 2, 2021
Exploring the Characteristics of Carbon Structures Obtained from LignoBoost Lignin
Adina Coroabă1,2, Irina Apostol1, Ioan Andrei Dascălu1
1"Petru Poni" Institute of Macromolecular Chemistry, Grigore Ghica Vodă 41 A, 700487 Iași, Romania.
Abstract:
In the present study, carbon structures from LignoBoost lignin were synthetized using HNO3/H2SO4 one-pot hydrothermal treatment, followed by a thermal treatment. The obtained compounds were characterized using different techniques, such as FTIR, DVS, DLS, XRD, fluorescence imaging and STEM. The formed LCMs presented graphitized structure with quasi-spherical shapes. All obtained materials presented negative values of zeta potential due to the charge from the hydroxyl and carboxyl groups, as confirmed by XPS analysis. All the data obtained sustained the heterogeneous composition of the lignin-based carbon materials, which arise from the complex structure of lignin. Fluorescence imaging demonstrated the potential of the materials as optical imaging agents.
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