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Updated: Sep 19, 2025

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
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Reflection grating fabrication for the Rockets for Extended-source X-ray Spectroscopy.

Drew M Miles1,2, Ross McCurdy2, Michael Labella3

  • 1Physics, Math, and Astronomy, California Institute of Technology, 1200 E. California Blvd., Pasadena, CA 91125 USA.

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Summary
This summary is machine-generated.

The Rockets for Extended-source X-ray Spectroscopy (tREXS) mission fabricated high-efficiency soft X-ray gratings using advanced nanofabrication. These gratings achieve over 70% efficiency, crucial for studying extended cosmic sources.

Keywords:
Electron beam lithographyReflection gratingsSuborbital rocketsSubstrate conformal imprint lithographyX-ray gratingsX-ray spectroscopy

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Area of Science:

  • X-ray astronomy
  • Astrophysical instrumentation
  • Nanofabrication

Background:

  • Soft X-ray spectroscopy is vital for studying extended astronomical sources.
  • Existing technologies faced limitations in grating efficiency and scalability.

Purpose of the Study:

  • To detail the nanofabrication of reflection gratings for the tREXS mission.
  • To demonstrate the production of high-efficiency gratings for soft X-ray spectroscopy.

Main Methods:

  • Electron-beam lithography (EBL) and KOH etching for master grating fabrication.
  • Substrate-conformal imprint lithography (SCIL) for mass replication of gratings.
  • Characterization of diffraction efficiency across the 0.18–0.8 keV band.

Main Results:

  • Achieved peak absolute diffraction efficiency >70% near 0.22 keV.
  • Demonstrated average absolute efficiency of ~50% across the 0.18–0.8 keV band.
  • Successfully replicated 191 gratings for the tREXS flight instrument.

Conclusions:

  • The developed nanofabrication and replication processes are suitable for producing high-performance X-ray gratings.
  • The tREXS gratings meet the requirements for sensitive soft X-ray spectroscopy of extended sources.
  • Future improvements can further enhance grating performance for astrophysical applications.